化工社化工社 化学情報印刷レポート · 研究参考用
Propyl isocyanate → 1-Propylcarbamoylcyclopropanesulfonamide tert-butylcarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Propyl isocyanate | HCID 61033 | — |
| 反応物 | 1-Methoxymethylcyclopropylsulfonylamine tert-butylcarbamate | HCID 66752382 | — |
| 生成物 | 1-Propylcarbamoylcyclopropanesulfonamide tert-butylcarbamate | HCID 66753294 | 100% |
反応手順
This compound was obtained in a crude 100% yield according to the procedure described for the synthesis of 1-methoxymethylcyclopropylsulfonylamine tert-butyl-carbamate except that 1.10 equivalents of n-propyl isocyanate was used as the electrophile. The compound was taken directly into the next reaction without purification: 1H NMR (CDCl3) δ 0.10 (m, 2H), 0.51 (m, 2H), 0.67 (m, 1H), 1.10 (m, 2H), 1.49 (s, 9H), 1.62 (m, 2H), 1.87 (d, J=7.0 Hz, 2H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07741281B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-d02dce065cef470d8f389fc3a6d68a94 |
| 出典メモ | uspto-grants-2010_06 |