2-Hydrazinopyridine → 3-TERT-BUTYL-1-(PYRIDIN-2-YL)-1H-PYRAZOL-5-AMINE

反応式

[N:1](O)=O.[CH3:4][C:5]([CH3:11])([CH3:10])[C:6](=O)[CH2:7][CH3:8].[NH:12]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][N:15]=1)[NH2:13]>>[C:5]([C:6]1[CH:7]=[C:8]([NH2:1])[N:12]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][N:15]=2)[N:13]=1)([CH3:11])([CH3:10])[CH3:4]

参加物

反応物 2

HCID 786452-Hydrazinopyridine

HCID 86603161HCID 86603161、化合物

生成物 1

HCID 433813303-TERT-BUTYL-1-(PYRIDIN-2-YL)-1H-PYRAZOL-5-AMINE収率 99%

実験手順

The title compound was prepared from 4,4-dimethyl-3-oxopentane nitrite and 2-hydrazinopyridine, using the same method as that described for preparation 7, as a solid in 99% yield.

後処理

customthat described for preparation 7, as a solid in 99% yield

出典と根拠

ORDレコード: ord-4126ddd95368497bb61a6425cfcd157f
出典データセット: uspto-grants-2009_03
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07511057B2

反応ノート

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