関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Butylimidazole | HCID 61347 | — |
| 反応物 | 1-(3-Bromopropyl)-4-methoxybenzene | HCID 12776996 | — |
| 生成物 | HCID 178448559 | HCID 178448559 | — |
反応手順
A mixture of 2.5 g (0.02 mole) of 1-butyl-1H-imidazole and 4.61 g (0.02 mole) of 1-(3-bromopropyl)-4-methoxybenzene is heated at 140° C. for about 1.5 hours. Follow the progress of the reaction by thin-layer chromatography on silica gel (methanol: 1M sodium chloride, 95:5). At the completion of the reaction, the cooled reaction product is triturated thoroughly with ether and on drying, provides the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04689341 |
|---|
| 出典データセット | uspto-grants-1987_08 |
|---|
| ORD ID | ord-713fc3bc0f894dfc920890737d051b18 |
|---|
| 出典メモ | uspto-grants-1987_08 |
|---|
