Methylamine → N-Methyl-2-(naphthalen-2-yl)acetamide
反応式
C([O:3][C:4](=O)[CH2:5][C:6]1[CH:15]=[CH:14][C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[CH:7]=1)C.[CH3:17][NH2:18]>>[CH3:17][NH:18][C:4](=[O:3])[CH2:5][C:6]1[CH:15]=[CH:14][C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[CH:7]=1参加物
3
実験手順
A mixture of naphthalen-2-yl-acetic acid ethyl ester (42.8 g, 200 mmol) and 64 mL of methylamine (40 wt % in H2O) were stirred at room temperature overnight. Then the white precipitate was filtered off and washed with water. After drying in vacuum the title compound was obtained as a white solid. MS (ES+): 226 (M+H)+.
後処理
- filtrationThen the white precipitate was filtered off
- washwashed with water
- dry with materialAfter drying in vacuum the title compound
- customwas obtained as a white solid
出典と根拠
- ORDレコード
- ord-34a9a8e5aed2438f8ffd075b5dd84221
- 出典データセット
- uspto-grants-2006_04
- 特許番号
- US07026326B2
反応ノート
読み込み中…