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Morpholine-3,5-dione → 4-[2-(2-Bromophenyl)ethyl]morpholine-3,5-dione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Morpholine-3,5-dione | HCID 364836 | — |
| 反応物 | 2-(2-Bromophenyl)ethan-1-ol | HCID 2734089 | — |
| 反応物 | 3-[2-(2-Bromophenyl)ethyl]-1-methylimidazolidine-2,4-dione | HCID 9857394 | — |
| 生成物 | 4-[2-(2-Bromophenyl)ethyl]morpholine-3,5-dione | HCID 9879306 | — |
反応手順
2-Bromophenethyl alcohol (402 mg, 2 mmol) and morpholine-3,5-dione (322 mg, 2.8 mmol) were treated as described in the preparation of compound 436. Purification was done by flash chromatography (petroleum ether/ethyl acetate 4:1) to provide the title compound as a colorless solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07034015B2 |
| 出典データセット | uspto-grants-2006_04 |
| ORD ID | ord-436f54ac426e448aa060a1c0a459eee7 |
| 出典メモ | uspto-grants-2006_04 |