反応式
[F:1][C:2]([F:20])([F:19])[C:3]1[CH:18]=[CH:17][C:6]([O:7][C:8]2[CH:16]=[CH:15][C:11]([C:12]([OH:14])=O)=[CH:10][CH:9]=2)=[CH:5][CH:4]=1.[NH2:21][CH2:22][C:23]([OH:25])=[O:24]>>[F:19][C:2]([F:1])([F:20])[C:3]1[CH:4]=[CH:5][C:6]([O:7][C:8]2[CH:9]=[CH:10][C:11]([C:12]([NH:21][CH2:22][C:23]([OH:25])=[O:24])=[O:14])=[CH:15][CH:16]=2)=[CH:17][CH:18]=1参加物
3
実験手順
A reaction similar to that described in Example 1 (1b) was conducted using 4-[4-(trifluoromethyl)phenoxy]benzoic acid (compound described in International Publication No. WO 04/14844, 7.06 g, 25.0 mmol) and glycine (1.88 g, 25.0 mmol) to give 8.38 g of the title compound (white powder, yield: 99%).
後処理
- customA reaction similar to
出典と根拠
- ORDレコード
- ord-509ebf9b6b8b4dfd84687b7bc7dade7a
- 出典データセット
- uspto-grants-2013_01
- 特許番号
- US08344029B2
関連ノート
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