化工社化工社 化学情報印刷レポート · 研究参考用
Ethynylcyclohexane → 2-cyclohexyl-5-methyl-7-nitro-1H-indole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethynylcyclohexane | HCID 70263 | — |
| 反応物 | 2-Iodo-4-methyl-6-nitroaniline | HCID 19735199 | — |
| 生成物 | 2-cyclohexyl-5-methyl-7-nitro-1H-indole | HCID 68634331 | 62.4% |
反応手順
6-Iodo-4-methyl-2-nitroaniline (500 mg, 1.8 mmol) and cyclohexylacetylene (0.23 ml, 1.8 mmol) were reacted according to the same procedure as Preparation 19 to give the title compound (290 mg, Yield 62%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08349885B2 |
| 出典データセット | uspto-grants-2013_01 |
| ORD ID | ord-757b1467e67e408fb9f30e363d61e28a |
| 出典メモ | uspto-grants-2013_01 |