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Hydrochloric Acid → propan-2-yl (2S)-2-amino-3-phenylpropanoate hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | L-Tyrosine | HCID 6057 | — |
| 反応物 | L-Phenylalanine | HCID 6140 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | propan-2-yl (2S)-2-amino-3-phenylpropanoate hydrochloride | HCID 15599949 | — |
| 生成物 | propan-2-yl (2S)-2-amino-3-(4-hydroxyphenyl)propanoate hydrochloride | HCID 67262861 | — |
反応手順
Excess HCl gas was added with stirring to a suspension of L-phenylalanine or L-tyrosine in excess isopropanol. The mixture was heated to reflux for 16 h, and then the volatiles were evaporated under vacuum to give L-phenylalanine isopropyl ester hydrochloride or L-tyrosine isopropyl ester hydrochloride of sufficient purity for immediate use.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07741328B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-733fefb0a17c4d6aa12ad2ef65fce39e |
| 出典メモ | uspto-grants-2010_06 |