関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Isopropanol | HCID 3776 | — |
| 反応物 | Diisopropylamine | HCID 7912 | — |
| 反応物 | 2-Chloropyrimidine | HCID 74404 | — |
| 生成物 | 2-Isopropoxypyrimidine | HCID 22138853 | — |
反応手順
A 2-chloropyrimidine was dissolved in isopropyl alcohol to which was added diisopropylamine. The reaction was heated in a sealed tube for ten days at 130° C. The cooled reaction mixture was concentrated, and the product purified via silica gel column chromatography to yield the 2-isopropoxypyrimidine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07741328B2 |
|---|
| 出典データセット | uspto-grants-2010_06 |
|---|
| ORD ID | ord-5eeae7a57a0340a0ac9a97edec8fd5c5 |
|---|
| 出典メモ | uspto-grants-2010_06 |
|---|
