Glycine tert-butyl ester → HCID 178443624、化合物
反応式
[C:1]([O:5][C:6](=[O:9])[CH2:7][NH2:8])([CH3:4])([CH3:3])[CH3:2].[CH3:10][C:11]([CH3:18])([CH:15]([CH3:17])[CH3:16])[CH2:12][CH:13]=O>C(Cl)Cl>[C:1]([O:5][C:6](=[O:9])[CH2:7]/[N:8]=[CH:13]/[CH2:12][C:11]([CH3:18])([CH3:10])[CH:15]([CH3:17])[CH3:16])([CH3:4])([CH3:3])[CH3:2]参加物
4
実験手順
Step D In a manner similar to the method described in Example 1a, glycine tert-butyl ester (1 g, 7.7 mmol) was reacted with 3,3,4-trimethyl-pentanal (1.1 g, 8 mmol) in CH2Cl2 at room temperature for 5 h to give [3,3,4-trimethyl-pent-(E)-ylideneamino]-acetic acid tert-butyl ester as a colorless oil (1.5 g, 80%).
出典と根拠
- ORDレコード
- ord-110f75357df64c9490e40fd8f9ab3abb
- 出典データセット
- uspto-grants-2013_01
- 特許番号
- US08354444B2
反応ノート
読み込み中…