Glycine tert-butyl ester → HCID 178451250、化合物
反応式
[C:1]([O:5][C:6](=[O:9])[CH2:7][NH2:8])([CH3:4])([CH3:3])[CH3:2].[CH:10]1([C:13]([CH3:18])([CH3:17])[CH2:14][CH:15]=O)[CH2:12][CH2:11]1>C(Cl)Cl>[C:1]([O:5][C:6](=[O:9])[CH2:7]/[N:8]=[CH:15]/[CH2:14][C:13]([CH:10]1[CH2:12][CH2:11]1)([CH3:18])[CH3:17])([CH3:4])([CH3:3])[CH3:2]参加物
4
実験手順
Step E In a manner similar to the method described in Example 1a, glycine tert-butyl ester (0.65 g, 5 mmol) was reacted with 3-cyclopropyl-3-methyl-butyraldehyde (0.68 g, 5.3 mmol) in CH2Cl2 at room temperature for 5 h to give [3-cyclopropyl-3-methyl-but-(E)-ylideneamino]-acetic acid tert-butyl ester as a colorless oil (0.9 g, 75%).
出典と根拠
- ORDレコード
- ord-9da494f0bd394f649ac9e42c88b302a0
- 出典データセット
- uspto-grants-2013_01
- 特許番号
- US08354444B2
反応ノート
読み込み中…