1-(3-Methylphenyl)cyclopropane-1-carbonitrile → m-Methylphenylacetonitrile

HRID 1810845ノート

反応式

HRID 1810845 の反応式
[C:1]1([CH3:12])[CH:6]=[CH:5][CH:4]=[C:3]([C:7]2([C:10]#[N:11])CC2)[CH:2]=1>CC(=O)OCC>[C:1]1([CH3:12])[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][C:10]#[N:11])[CH:2]=1

参加物

3

反応物 1

HCID 200261921-(3-Methylphenyl)cyclopropane-1-carbonitrile

生成物 1

HCID 76279m-Methylphenylacetonitrile

試薬・触媒・溶媒 1

HCID 8857Ethyl Acetate溶媒

実験手順

After silica gel chromatography of the residue (HEP/EA gradient), an approximately 1:1 mixture of 1-m-tolyl-cyclopropanecarbonitrile and the starting compound m-tolylacetonitrile was obtained.

出典と根拠

ORDレコード
ord-d36e32e663a04088b27bc5b2a8a16806
出典データセット
uspto-grants-2013_01
特許番号
US08362073B2

反応ノート

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