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Dabsyl chloride → 1-(2-{1-[4-(4-Dimethylaminophenylazo)benzenesulfonyl]piperidin-4-yl}ethyl)-2-(ethoxymethyl)-6,7-dimethyl-1h-imidazo[4,5-c]pyridin-4-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dabsyl chloride | HCID 91660 | — |
| 反応物 | 2-(ethoxymethyl)-6,7-dimethyl-1-(2-piperidin-4-ylethyl)-1H-imidazo[4,5-c]pyridin-4-amine | HCID 12972962 | — |
| 生成物 | 1-(2-{1-[4-(4-Dimethylaminophenylazo)benzenesulfonyl]piperidin-4-yl}ethyl)-2-(ethoxymethyl)-6,7-dimethyl-1h-imidazo[4,5-c]pyridin-4-amine | HCID 10312362 | — |
反応手順
Using the method of Examples 49-56, 4-dimethylaminoazobenzene-4′-sulfonyl chloride was reacted with 2-(ethoxymethyl)-6,7-dimethyl-1-(2-piperidin-4-ylethyl)-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired product. The observed accurate mass was 619.3185.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06878719B2 |
| 出典データセット | uspto-grants-2005_04 |
| ORD ID | ord-ff65ba1fff1a4832952168078b0adb09 |
| 出典メモ | uspto-grants-2005_04 |