化工社化工社 化学情報印刷レポート · 研究参考用
1,2-Dichlorobenzene → 7-Allyl-1H-indazol-6-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Dichlorobenzene | HCID 7239 | — |
| 反応物 | 6-Allyloxy-1H-indazole | HCID 22496569 | — |
| 生成物 | 7-Allyl-1H-indazol-6-ol | HCID 135843647 | 60% |
反応手順
A solution of the product from Step A (14.2 g, 82 mmol) in 1,2-dichlorobenzene (90 mL) was fluxed for 6 h and the reaction mixture was evaporated to a residue which was purified by chromatography (silica, EtOAc) to give a tan solid (8.59 g, 60%) that was used in the next step: LC/MS (+APCI) m/z 175 (M+H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06881749B2 |
| 出典データセット | uspto-grants-2005_04 |
| ORD ID | ord-36faabe96ce14c83ab09362c11ff1eb9 |
| 出典メモ | uspto-grants-2005_04 |