化工社化工社 化学情報印刷レポート · 研究参考用
Methyl iodide → (2,3-Dimethoxyphenyl)(phenyl)methanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl iodide | HCID 6328 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | Sulisobenzone | HCID 19988 | — |
| 生成物 | (2,3-Dimethoxyphenyl)(phenyl)methanone | HCID 13270875 | — |
反応手順
In Scheme II, benzophenone 4 was treated with iodomethane in the presence of potassium carbonate to produce the dimethoxy-benzophenone 7. Bromination of 7 with bromine in chloroform furnished bromo-benzophenone 8, which was converted to benizisoxazole 9 according to Scheme I.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06884814B2 |
| 出典データセット | uspto-grants-2005_04 |
| ORD ID | ord-103c406b5aa941edb3000b629ec4d5b6 |
| 出典メモ | uspto-grants-2005_04 |