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3-Methoxypropylamine → (7-Bromo-3-nitroquinolin-4-yl)-(3-methoxypropyl)amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Methoxypropylamine | HCID 1672 | — |
| 反応物 | 7-Bromo-4-chloro-3-nitroquinoline | HCID 21984361 | — |
| 生成物 | (7-Bromo-3-nitroquinolin-4-yl)-(3-methoxypropyl)amine | HCID 21984327 | 94.2% |
反応手順
7-Bromo-4-chloro-3-nitroquinoline (29.54 g, 102.7 mmol) was reacted with 3-methoxy propyl amine (10.07 g, 113.0 mmol) according to the method described in Part A of Examples 125-135 to provide 32.9 g of (7-bromo-3-nitroquinolin-4-yl)-(3-methoxypropyl)amine as a yellow solid. The product was not recrystallized.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07598382B2 |
| 出典データセット | uspto-grants-2009_10 |
| ORD ID | ord-0577e3a026534b0f825b9a02214d4dce |
| 出典メモ | uspto-grants-2009_10 |