4-Methoxybenzaldehyde → S-ethyl (E)-3-(4-methoxyphenyl)prop-2-enethioate
反応式
COc1ccc(C=O)cc1.CCSC(=O)CC(=O)O>NCc1ccccc1.O=C(O)C(F)(F)F.CN(C)c1ccncc1.CN(C)C=O>CCSC(=O)/C=C/c1ccc(OC)cc1参加物
6
反応条件
- 温度
- 25 °C
後処理
- temperatureThe product mixture was cooled to 25 °C.
- filtrationFiltered through a pad of celite · Organic 相を保持
- wash"The celite was washed with ethyl acetate (3 x 1 mL)."
- concentrationThe filtrate was concentrated under reduced pressure
- additionA 0.07 M stock solution of the internal standard ethylene carbonate (0.70 mL in CDCl3) was added.
出典と根拠
- ORDレコード
- ord-d98c486ba3ae4b90868aae8de0a673dc
- 出典データセット
- Bayesian optimization of 5 decarboxylative olefination reactions
反応ノート
読み込み中…