化工社化工社 化学情報印刷レポート · 研究参考用
Tributylamine → 5-Butoxy-4-methyl-1,3-oxazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tributylamine | HCID 7622 | — |
| 反応物 | n-Butyl alpha-isocyanopropionate | HCID 11171108 | — |
| 溶媒 | Chlorobenzene | HCID 7964 | — |
| 生成物 | 5-Butoxy-4-methyl-1,3-oxazole | HCID 9877440 | — |
反応手順
A continuously operated dividing wall column (4.8 m×64 mm) packed with 3×3 mm V2A Raschig rings and a dividing wall of height 2.4 m having 60 theoretical plates was charged with a mixture of 13.1% by weight of n-butyl α-isocyanopropionate (R1=n-butyl, R2=methyl), 32.2% by weight of monochlorobenzene and 50.1% by weight of tri-n-butylamine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07038058B2 |
| 出典データセット | uspto-grants-2006_05 |
| ORD ID | ord-5d92cae410694a43864bb8ca79139d29 |
| 出典メモ | uspto-grants-2006_05 |