化工社化工社 化学情報印刷レポート · 研究参考用
Piperidine → 4-Piperidinylbut-1-ene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Piperidine | HCID 8082 | — |
| 反応物 | Homoallyl bromide | HCID 21241 | — |
| 生成物 | 4-Piperidinylbut-1-ene | HCID 4562282 | 93.4% |
反応手順
4-Bromobut-1-ene (1.35 g) was treated with piperidine (1.7 g) and heated at reflux for 3 hours. The mixture was cooled to ambient temperature, filtered and the residue washed with ether (50 mL). The combined filtrate and washings were evaporated to give the title compound (1.3 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07041827B2 |
| 出典データセット | uspto-grants-2006_05 |
| ORD ID | ord-adb29397f4884d54a3b13354f001a0f2 |
| 出典メモ | uspto-grants-2006_05 |