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HRID 1824547作成日:2026年10月27日

Piperidine → 4-Piperidinylbut-1-ene

https://huagongshe.com/reaction/1824547

反応式

関与物質

役割名称HCID仕込み量
反応物PiperidineHCID 8082—
反応物Homoallyl bromideHCID 21241—
生成物4-Piperidinylbut-1-eneHCID 456228293.4%

反応手順

4-Bromobut-1-ene (1.35 g) was treated with piperidine (1.7 g) and heated at reflux for 3 hours. The mixture was cooled to ambient temperature, filtered and the residue washed with ether (50 mL). The combined filtrate and washings were evaporated to give the title compound (1.3 g).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07041828B2
出典データセットuspto-grants-2006_05
ORD IDord-5c51527d0b6f4cf0b91aba41d78fbf5c
出典メモuspto-grants-2006_05