化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → 2-[4-Hydroxyphenyl]-8-methylimidazo[1,2-a]pyridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | 2-Bromo-1-(4-hydroxyphenyl)ethanone | HCID 4964 | — |
| 反応物 | 2-Aminopicoline | HCID 66824522 | — |
| 生成物 | 2-[4-Hydroxyphenyl]-8-methylimidazo[1,2-a]pyridine | HCID 22015659 | — |
反応手順
The product of step A (30 g) and 2-aminopicoline (15 mL) in ethanol (200 mL) was heated at reflux temperature for 4 hours then cooled to ambient temperature. The resulting precipitate containing the title compound was isolated via filtration (27 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07041828B2 |
| 出典データセット | uspto-grants-2006_05 |
| ORD ID | ord-2edc2c97acd44593b558775a90e45be7 |
| 出典メモ | uspto-grants-2006_05 |