2-Nitrobenzenesulfonamide → N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-2-nitro-benzenesulfonamide

関与物質

役割	名称	HCID	仕込み量
反応物	2-Nitrobenzenesulfonamide	HCID 138510	—
反応物	3-[4-(Z)-(1,2-diphenylbut-1-enyl)phenyl]-acrylic acid	HCID 3036152	—
生成物	N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-2-nitro-benzenesulfonamide	HCID 69781207	—

反応手順

Prepared by coupling 1a and 2-nitrobenzenesulfonamide in accordance with Procedure 1, Method B described hereinabove. Yield (22%); 1H NMR (d6-DMSO) δ 8.18 (d, J=5.2 Hz, 1H), 7.99 (d, J=5.9 Hz, 1H), 7.94–7.84 (m, 2H), 7.44–7.08 (m, 13H), 6.86 (d, J=8.1 Hz, 2H), 6.50 (d, J=15.7 Hz, 1H), 2.36 (q, J=7.4 Hz, 2H), 0.82 (t, J=7.4 Hz, 3H); APcI m/z: 539 (M+H+).

情報源と証拠

DOI	10.6084/m9.figshare.5104873.v1
特許番号	US07045540B2
出典データセット	uspto-grants-2006_05
ORD ID	ord-9abc4a094bfe44e1b5660abb4bab97eb
出典メモ	uspto-grants-2006_05