Butanal → 56249-61-7

HRID 1828213ノート

反応式

HRID 1828213 の反応式
[CH:1](=O)[CH2:2][CH2:3][CH3:4].[CH2:6]([NH2:13])[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1>C1(C)C=CC=CC=1>[CH:1](=[N:13][CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[CH2:2][CH2:3][CH3:4]

参加物

4

反応物 2

HCID 261ButanalHCID 7504Benzylamine

生成物 1

HCID 455591156249-61-7

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

This material is a known compound prepared in the standard fashion. To about 100 mL of toluene was added 28 mL of butyraldehyde, 34 mL of benzylamine, and several grams of 3A molecular sieves. The mixture became warm and turbid after standing for a few minutes. After standing for several hours the mixture was colorless and transparent. The imine product was isolated by distillation under vacuum and characterized by NMR spectroscopy.

後処理

  1. customprepared in the standard fashion
  2. temperatureThe mixture became warm
  3. waitafter standing for a few minutes
  4. waitAfter standing for several hours

出典と根拠

ORDレコード
ord-7e2557d71c324fc2afdd4937f6cdf32b
出典データセット
uspto-grants-2006_06
特許番号
US07056979B1

反応ノート

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