関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 4-tert-Butylcyclohexanol | HCID 7391 | — |
| 反応物 | Potassium bisulfate | HCID 516920 | — |
| 反応物 | ethylacetate KHSO4 | HCID 86585043 | — |
| 生成物 | 4-Tert-butylcyclohex-1-ene | HCID 16688 | — |
反応手順
20 g 4-t-butyl-1-cyclohexanol are mixed with 17 g KHSO4 and stirred for one week at 95° C. After the addition of ethylacetate KHSO4 is filtered off. Ethylacetate is evaporated and the product obtained by fractional distillation.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07057059B2 |
|---|
| 出典データセット | uspto-grants-2006_06 |
|---|
| ORD ID | ord-af0b71c7642b4961a781a860d53df6c6 |
|---|
| 出典メモ | uspto-grants-2006_06 |
|---|
