3-Formyl-2-methylindole → HCID 22139069、化合物

反応式

[CH3:1][C:2]1([CH3:13])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]([CH:11]=O)[CH2:3]1.C[C:15]1[NH:16]C2C(C=1C=O)=CC=CC=2>>[CH3:1][C:2]1([CH3:13])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]([CH2:11][NH:16][CH3:15])[CH2:3]1

参加物

反応物 2

HCID 731663-Formyl-2-methylindole

HCID 221390871,1-dimethyl-3H-indene-3-carboxaldehyde

生成物 1

HCID 22139069HCID 22139069、化合物収率 81%

実験手順

According to the procedure of Preparation 12, except substituting 1,1-dimethyl-3H-indene-3-carboxaldehyde for the 2-methylindole-3-carboxaldehyde, the title compound (3 g, 81%) was obtained as a reddish oil: MS (ES) m/e 188.2 (M+H)+.

後処理

customAccording to the procedure of Preparation 12

出典と根拠

ORDレコード: ord-09fd2a8ab4004f9185b7f0fdd33bf3d7
出典データセット: uspto-grants-2010_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07741339B2

反応ノート

読み込み中…