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3-Formyl-2-methylindole → methyl 1-methyl-3-(methylaminomethyl)-1H-indole-7-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Formyl-2-methylindole | HCID 73166 | — |
| 反応物 | Methyl 3-formyl-1-methylindole-7-carboxylate | HCID 22139012 | — |
| 生成物 | methyl 1-methyl-3-(methylaminomethyl)-1H-indole-7-carboxylate | HCID 22139141 | 92% |
反応手順
According to the procedure of Preparation 12, except substituting 1-methyl-7-methoxycarbonyl-1H-indole 3-carboxaldehyde for the 2-methylindole-3-carboxaldehyde, the title compound (1.7 g, 92%) was obtained as an oil: MS (ES) m/e 233.2 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07741339B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-ef4a20eef7314d66a3e37f69970bbd2f |
| 出典メモ | uspto-grants-2010_06 |