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4-Sulfamoylthiobenzamide → 4-[5-Methyl-4-(4-methylpyridin-3-yl)-1,3-thiazol-2-yl]benzenesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Sulfamoylthiobenzamide | HCID 3003266 | — |
| 反応物 | 2-Bromo-1-(4-methylpyridin-3-yl)propan-1-one | HCID 22049762 | — |
| 生成物 | 4-[5-Methyl-4-(4-methylpyridin-3-yl)-1,3-thiazol-2-yl]benzenesulfonamide | HCID 22049755 | 56.8% |
反応手順
By the reaction in the same manner as in Example 25-iii) using 2-bromo-1-(4-methylpyridin-3-yl)propan-1-one hydrobromate (510 mg) and 4-(aminosulfonyl)benzenecarbothioamide (355 mg), the title compound (322 mg) was obtained as colorless powder crystals.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07067537B2 |
| 出典データセット | uspto-grants-2006_06 |
| ORD ID | ord-ce545a3b15d4460abeb2f3e5f13ee968 |
| 出典メモ | uspto-grants-2006_06 |