2,4-Dichlorobenzoyl chloride → HCID 178491588、化合物
反応式
ClC1C=C(Cl)C=CC=1[C:4](Cl)=[O:5].Cl[C:13]1[CH:28]=[CH:27][C:16]([C:17]([NH:19][C:20]2[CH:21]=[N:22][C:23]([OH:26])=[CH:24][CH:25]=2)=[O:18])=[CH:15][CH:14]=1>>[OH:26][C:23]1[N:22]=[CH:21][C:20]([NH:19][C:17](=[O:18])[C:16]2[CH:27]=[CH:28][C:13]([O:5][CH3:4])=[CH:14][CH:15]=2)=[CH:25][CH:24]=1参加物
3
実験手順
Starting from 2,4-dichlorobenzoyl chloride (2.10 g, 10.0 mmol) and using the procedure as described for the preparation of 4-Chloro-N-(6-hydroxy-pyridin-3-yl)-benzamide yielded the title compound, which was used without further purification.
出典と根拠
- ORDレコード
- ord-830003a4046240df9a32526f044fa683
- 出典データセット
- uspto-grants-2006_06
- 特許番号
- US07067517B2
反応ノート
読み込み中…