化工社化工社 化学情報印刷レポート · 研究参考用
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic Acid 4-hydroxymethyl-pyrazol-1-yl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| 反応物 | 1-Hydroxy-4-hydroxymethylpyrazole | HCID 22047685 | — |
| 生成物 | Methyl-phenyl-carbamic Acid 4-hydroxymethyl-pyrazol-1-yl Ester | HCID 69517970 | — |
反応手順
The title compound was prepared from 1-hydroxy-4-hydroxymethylpyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (62%, oil).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07067517B2 |
| 出典データセット | uspto-grants-2006_06 |
| ORD ID | ord-b88859a656dc439996cc7e400ae7589d |
| 出典メモ | uspto-grants-2006_06 |