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2-Butanamine, 1-methoxy- → [4-(2,4-Dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1-methoxymethyl-propyl)-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Butanamine, 1-methoxy- | HCID 93837 | — |
| 反応物 | 2-Chloro-4-(2,4-dichloro-phenyl)-3-nitro-pyridine | HCID 22052102 | — |
| 生成物 | [4-(2,4-Dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1-methoxymethyl-propyl)-amine | HCID 22052219 | 88% |
反応手順
2-Chloro-4-(2,4-dichloro-phenyl)-3-nitro-pyridine (0.20 g, 0.66 mmol) and 1-methoxymethyl-propylamine (0.14 g, 1.32 mmol) were treated as in Part D of Example 9 to yield 0.21 g (88%) of [4-(2,4-dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1-methoxymethyl-propyl)-amine: MS (AP) m/z 370.2 [(M+H)+, 97].
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07067658B2 |
| 出典データセット | uspto-grants-2006_06 |
| ORD ID | ord-0cb88146fb7d431c84f6f9f0b98a05c9 |
| 出典メモ | uspto-grants-2006_06 |