N-(1-pyridin-4-ylethyl)formamide → HCID 22052374、化合物

HRID 1831807ノート

反応式

HRID 1831807 の反応式
[N:1]1[CH:6]=[CH:5][C:4]([CH:7]([NH:9][CH:10]=[O:11])[CH3:8])=[CH:3][CH:2]=1.[H][H]>C(O)(=O)C>[NH:1]1[CH2:6][CH2:5][CH:4]([CH:7]([NH:9][CH:10]=[O:11])[CH3:8])[CH2:3][CH2:2]1

参加物

4

反応物 2

HCID 2771720N-(1-pyridin-4-ylethyl)formamideHCID 178418361HCID 178418361、化合物

生成物 1

HCID 22052374HCID 22052374、化合物

試薬・触媒・溶媒 1

HCID 176Acetic Acid溶媒

実験手順

N-(1-Pyridin-4-yl-ethyl)-formamide (1.86 g, 12.38 mmol) was dissolved in 50 ml of acetic acid. After addition of Rh (5% on Al2O3, 307 mg) the mixture was hydrogenated with 10 bar hydrogen and 100° C. for 120 hours. The mixture was evaporated and lyophilised. The crude material was used without purification.

後処理

  1. customThe mixture was evaporated
  2. customThe crude material was used without purification

出典と根拠

ORDレコード
ord-e9ad8eb38b184374bd02bcba4d2cf473
出典データセット
uspto-grants-2006_06
特許番号
US07067665B2

反応ノート

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