Dichloromethane → HCID 22765685、化合物
反応式
Cl.[CH2:2]([NH:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH:3]=[CH2:4].C(Cl)Cl.[Cl:13][CH:14]([Cl:18])[C:15](Cl)=[O:16]>C(N(CC)CC)C>[CH2:2]([N:5]([CH2:6][CH2:7][CH2:8][CH3:9])[C:15](=[O:16])[CH:14]([Cl:18])[Cl:13])[CH:3]=[CH2:4]参加物
5
実験手順
Ten and five-tenths grams of allyl-n-butyl amine hydrochloride was added to 100 ml. of methylene chloride followed by 14.5 g. of triethylamine. The mixture was stirred in a water bath at room temperature while 10.4 g. of dichloroacetyl chloride was added dropwise, and stirring was continued for 30 minutes after addition was complete. The mixture was washed and the solvent stripped under vacuum. Yield was 13 g., nD30 1.4603. The intermediate was used without further purification to prepare Compound No. 12 (Example VII).
後処理
- stirringstirring
- additionafter addition
- washThe mixture was washed
- customThe intermediate was used without further purification
- customto prepare Compound No
出典と根拠
- ORDレコード
- ord-c4f6d65782d343dfbad6f8dc53dc3ced
- 出典データセット
- uspto-grants-1978_01
- 特許番号
- US04069038
反応ノート
読み込み中…