Hydrochloric Acid → HCID 178526618、化合物
反応式
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]2[N:13]=[CH:14][N:15](C(C3C=CC=CC=3)(C3C=CC=CC=3)C3C=CC=CC=3)[CH:16]=2)[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].Cl>CO>[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]2[N:13]=[CH:14][NH:15][CH:16]=2)[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2]参加物
4
実験手順
A mixture of 11 g of the product obtained in Step 3, 6 ml of concentrated hydrochloric acid and 150 ml of methanol is heated at reflux for 2 hours. The solvent is concentrated and the residue is taken up in an isopropanol/diethyl ether mixture. The expected product is obtained by filtering off the precipitate that has formed.
後処理
- temperatureis heated
- temperatureat reflux for 2 hours
- concentrationThe solvent is concentrated
出典と根拠
- ORDレコード
- ord-0af9401dae884228ac9b80e269f20f5d
- 出典データセット
- uspto-grants-2004_08
- 特許番号
- US06784183B2
反応ノート
読み込み中…