化工社化工社 化学情報印刷レポート · 研究参考用
Uracil → Benzyl chloromethyl ether
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Uracil | HCID 1174 | — |
| 反応物 | 7-Methylxanthine | HCID 68374 | — |
| 反応物 | 2-Chloromethyl 2-(trimethylsilyl)ethyl ether | HCID 2724271 | — |
| 生成物 | Benzyl chloromethyl ether | HCID 137983 | — |
反応手順
In a similar manner to the procedures described in Reference Example 3, reactions were carried out using 7-methylxanthine, instead of pyrimidine-2,4-dione, and using 2-(trimethylsilyl)ethoxymethyl chloride, instead of benzyloxymethyl chloride, to give the title compound (yield 69%) as a pale yellow powder.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06673804B1 |
| 出典データセット | uspto-grants-2004_01 |
| ORD ID | ord-aabbc1fe7b634686ad862928f82d70f5 |
| 出典メモ | uspto-grants-2004_01 |