Potassium Carbonate → HCID 178482267、化合物
反応式
F[C:2]1[CH:3]=[CH:4][C:5]([N+:10]([O-:12])=[O:11])=[C:6]([CH:9]=1)[NH:7][CH3:8].[CH3:13][C:14]1[N:19]=[C:18]([OH:20])[CH:17]=[C:16]([OH:21])[CH:15]=1.C(=O)([O-])[O-].[K+].[K+]>CN(C=O)C>[CH3:13][C:14]1[N:19]=[C:18]([OH:20])[CH:17]=[C:16]([O:21][C:2]2[CH:3]=[CH:4][C:5]([N+:10]([O-:12])=[O:11])=[C:6]([NH:7][CH3:8])[CH:9]=2)[CH:15]=1参加物
5
実験手順
The reaction and post-treatment were carried out according to Example (16c) using 5-fluoro-N-methyl-2-nitroaniline (US2003-675927, 6.30 g, 37.0 mmol), 6-methylpyridine-2,4-diol (5.09 g, 40.7 mmol), potassium carbonate (5.63 g, 40.7 mmol) and DMF (100 mL) to obtain the title compound (9.06 g, 89%) as a yellow solid.
後処理
- customThe reaction
出典と根拠
- ORDレコード
- ord-08dc45ac78a04345bec8abf2f99cbcd8
- 出典データセット
- uspto-grants-2015_02
- 特許番号
- US08946264B2
反応ノート
読み込み中…