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Xanthine → Naphthalene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Xanthine | HCID 1188 | — |
| 反応物 | Theophylline | HCID 2153 | — |
| 反応物 | Caffeine | HCID 2519 | — |
| 反応物 | Paraxanthine | HCID 4687 | — |
| 反応物 | Theobromine | HCID 5429 | — |
| 反応物 | Acetylacetone | HCID 31261 | — |
| 反応物 | 7-Methylxanthine | HCID 68374 | — |
| 反応物 | 3-Methylxanthine | HCID 70639 | — |
| 反応物 | Ammonium Acetate | HCID 517165 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | Naphthalene | HCID 931 | — |
反応手順
Chemicals. Caffeine, theophylline, theobromine, paraxanthine, 7-methylxanthine, 3-methylxanthine, xanthine, ammonium acetate, acetic acid, 2,4-pentanedione, spinach ferredoxin reductase, and spinach ferredoxin were purchased from Sigma-Aldrich. Reductase and ferredoxin of Pseudomonas sp. 9816 naphthalene dioxygenase were kindly provided by Dr. David T. Gibson. Soytone was obtained from Becton, Dickinson and Company. High-pressure liquid chromatography (HPLC)-grade methanol (J. T. Baker) was used in chromatographic studies.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08951752B2 |
| 出典データセット | uspto-grants-2015_02 |
| ORD ID | ord-34627c36c7084bd1be335f8d306d814e |
| 出典メモ | uspto-grants-2015_02 |