Acetic Acid → 2,7-dimethyl-3H-benzimidazol-5-ol
反応式
[NH2:1][C:2]1[CH:3]=[C:4]([OH:10])[CH:5]=[C:6]([CH3:9])[C:7]=1[NH2:8].[C:11](O)(=O)[CH3:12]>>[CH3:11][C:12]1[NH:1][C:2]2[CH:3]=[C:4]([OH:10])[CH:5]=[C:6]([CH3:9])[C:7]=2[N:8]=1参加物
3
実験手順
0.553 g (4.00 mml) 3,4-diamino-5-methyl-phenol in 5.00 mL glacial acetic acid were boiled for 3 h. Then the reaction mixture was evaporated down and dried under HV.
後処理
- customThen the reaction mixture was evaporated down
- customdried under HV
出典と根拠
- ORDレコード
- ord-78ab22a252eb429682514ead839f265e
- 出典データセット
- uspto-grants-2015_02
- 特許番号
- US08952014B2
反応ノート
読み込み中…