Methoxyacetic Acid → 2-(methoxymethyl)-4-methyl-1H-benzo[d]imidazol-6-ol
反応式
[NH2:1][C:2]1[CH:3]=[C:4]([OH:10])[CH:5]=[C:6]([CH3:9])[C:7]=1[NH2:8].[CH3:11][O:12][CH2:13][C:14](O)=O>>[CH3:11][O:12][CH2:13][C:14]1[NH:1][C:2]2[CH:3]=[C:4]([OH:10])[CH:5]=[C:6]([CH3:9])[C:7]=2[N:8]=1参加物
3
実験手順
0.55 g (4.00 mmol) 3,4-diamino-5-methyl-phenol and 1.57 mL (20.00 mmol) methoxy-acetic acid were stirred for 1 h at 120° C. Then the reaction mixture was evaporated down and further reacted as crude product.
後処理
- customThen the reaction mixture was evaporated down
- customfurther reacted as crude product
出典と根拠
- ORDレコード
- ord-0a9782ae3d6c474b9a96289133f1de66
- 出典データセット
- uspto-grants-2015_02
- 特許番号
- US08952014B2
反応ノート
読み込み中…