化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → Cyclohexanecarbonyl chloride, 5-methyl-2-(1-methylethyl)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | p-Menthane-3-carboxylic acid | HCID 97896 | — |
| 生成物 | Cyclohexanecarbonyl chloride, 5-methyl-2-(1-methylethyl)- | HCID 13734319 | — |
反応手順
Menthane-3-carboxylic acid (54.35 g) was refluxed with 80 ml of thionyl chloride for 3 hours. The SOCl2 was removed by distillation, and the acid chloride was distilled at 114-115° C. (8 Torr). (Lit. b.p. 84-85° C. at 3.5 Torr). Yield: 50 g (84%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07741355B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-34d4b82d37d54495b5bc982f2f768f38 |
| 出典メモ | uspto-grants-2010_06 |