化工社化工社 化学情報印刷レポート · 研究参考用
Aniline → 2-Butylmercaptoaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | o-Nitrobenzenethiol | HCID 21002 | — |
| 反応物 | 2-Pyrrolidinone, 1-(chloromethyl)- | HCID 2770497 | — |
| 生成物 | 2-Butylmercaptoaniline | HCID 10329960 | — |
反応手順
2-Butylmercaptoaniline was prepared from -2-nitrothiophenol by a two-step reaction sequence consisting of alkylation followed by reduction. The aniline then was condensed with N-chloromethyl-2-pyrrolidone to yield the desired product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04216152 |
| 出典データセット | uspto-grants-1980_08 |
| ORD ID | ord-af6436cd13f6470db1b7e8d2de179146 |
| 出典メモ | uspto-grants-1980_08 |