化工社化工社 化学情報印刷レポート · 研究参考用
Oct-2-ene → Methyl-undec-9-enoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Oct-2-ene | HCID 8126 | — |
| 反応物 | Methyl Oleate | HCID 5364509 | — |
| 生成物 | Methyl-undec-9-enoate | HCID 62588 | 5% |
反応手順
Reaction was carried out in the same manner as in Example 1, except that a mixture of 1 ml of methyl oleate and 1 ml of 2-octene was used in place of 1 ml of the methyl oleate, the reaction temperature was 70° C., and the reaction time was 17 hours. There were obtained methyl 9-undecenoate in a yield of about 5% and methyl 9-pentadecanoate in a yield of about 7% (estimated from the chromatogram). Besides, metathesis products were obtained independently from methyl oleate and 2-octene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04217299 |
| 出典データセット | uspto-grants-1980_08 |
| ORD ID | ord-2dd0dc184fc1498498593a91c8adadba |
| 出典メモ | uspto-grants-1980_08 |