化工社化工社 化学情報印刷レポート · 研究参考用
Sulfanilamide → 4-(2-Methyl-5-m-tolyl-pyrrol-1-yl)-benzenesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfanilamide | HCID 5333 | — |
| 反応物 | Methyl vinyl ketone | HCID 6570 | — |
| 反応物 | 3-Methylbenzaldehyde | HCID 12105 | — |
| 生成物 | 4-(2-Methyl-5-m-tolyl-pyrrol-1-yl)-benzenesulfonamide | HCID 68484259 | — |
反応手順
Meta-methylbenzaldehyde and but-3-en-2-one were treated according to the procedure outlined in General Procedure C followed by subjecting the resulting product to conditions outlined in General Procedure D along with p-aminosulfonyl phenylamine to obtain the titled compound. 1H NMR (CDCl3) δ ppm 2.15 (3H), 2.05 (3H), 4.90 (2H), 6.10 (1H), 6.30 (1H), 6.89-7.90 (8H); MS (ESI) m/z 327 (M+H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07741364B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-5c2fa4e2b03541a59abf59fc72cb1df7 |
| 出典メモ | uspto-grants-2010_06 |