関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Naphthylamine | HCID 7057 | — |
| 反応物 | Chlorosuccinimide | HCID 31398 | — |
| 溶媒 | Carbon Tetrachloride | HCID 5943 | — |
| 生成物 | 1-Chloro-naphthalen-2-ylamine | HCID 418014 | 96.2% |
反応手順
To a CCl4 (600 mL) solution of 2-naphthylamine (10 g) at 49° C. was added NCS (9.51 g, 1.02 eq) in portions. The mixture was stirred at 49° C. for 1.5 h then concentrated to dryness to give 1-chloro-2-naphthylamine (11.94 g, 96%) as a dark solid. MS Found: (M+H)+=178.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07625921B2 |
|---|
| 出典データセット | uspto-grants-2009_12 |
|---|
| ORD ID | ord-b3aa8510d4024a85bb81e219ef6b4778 |
|---|
| 出典メモ | uspto-grants-2009_12 |
|---|
