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3,4-Dichlorocinnamic acid → (Rac)-1-[(e)-3-(3,4-dichloro-phenyl)-acryloyl]-6-methyl-[1,4]diazepan-5-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,4-Dichlorocinnamic acid | HCID 688027 | — |
| 反応物 | 6-Methyl-1,4-diazepan-5-one hydrochloride | HCID 68434983 | — |
| 生成物 | (Rac)-1-[(e)-3-(3,4-dichloro-phenyl)-acryloyl]-6-methyl-[1,4]diazepan-5-one | HCID 68432289 | — |
反応手順
In analogy to the procedure described in intermediate 78C, (E)-3,4-dichlorocinnamic acid and 6-methyl-[1,4]diazepan-5-one hydrochloride gave the title compound as a colorless gum, MS: 327.1 (MH+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07632829B2 |
| 出典データセット | uspto-grants-2009_12 |
| ORD ID | ord-d5ecb3da94114dcea2c2af6b1d8127fb |
| 出典メモ | uspto-grants-2009_12 |