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4-Amino-2-(trifluoromethyl)benzonitrile → 1,1,1-Trifluoro-4-phenyl-2-[(4-cyano-3-(trifluoromethyl)phenyl)iminomethyl]-4-methylpentan-2-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Amino-2-(trifluoromethyl)benzonitrile | HCID 522170 | — |
| 反応物 | 2-Hydroxy-4-methyl-4-phenyl-2-trifluoromethylpentanal | HCID 17989092 | — |
| 生成物 | 1,1,1-Trifluoro-4-phenyl-2-[(4-cyano-3-(trifluoromethyl)phenyl)iminomethyl]-4-methylpentan-2-ol | HCID 17989176 | — |
反応手順
Analogously to Example 13, 120 mg of 2-hydroxy-4-methyl-4-phenyl-2-(trifluoromethyl)pentanal and 78 mg of 4-cyano-3-(trifluoromethyl)aniline are converted into 71 mg of product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07638515B2 |
| 出典データセット | uspto-grants-2009_12 |
| ORD ID | ord-a1976d7aafd44465b8a472d78d276dc6 |
| 出典メモ | uspto-grants-2009_12 |