2-(3,4-Dichloro-phenylamino)-propionic Acid → HCID 18341195、化合物

反応式

[CH3:1][NH:2][C:3](=[O:9])[C@H:4]([CH:6]([CH3:8])[CH3:7])[NH2:5].[Cl:10][C:11]1[CH:12]=[C:13]([NH:18][CH:19]([C:21](O)=[O:22])[CH3:20])[CH:14]=[CH:15][C:16]=1[Cl:17]>>[CH3:1][NH:2][C:3](=[O:9])[C@H:4]([CH:6]([CH3:8])[CH3:7])[NH:5][C:21](=[O:22])[CH:19]([CH3:20])[NH:18][C:13]1[CH:14]=[CH:15][C:16]([Cl:17])=[C:11]([Cl:10])[CH:12]=1

参加物

反応物 2

HCID 69164262-(3,4-Dichloro-phenylamino)-propionic Acid

HCID 11423608N-Methyl-L-valinamide

生成物 1

HCID 18341195HCID 18341195、化合物

実験手順

Following General Procedure D and using L-valine N-methyl amide (from Example E above) and N-(3,4-dichlorophenyl)-D,L-alanine (from Example A above), the title compound was prepared as a solid (mp=145-160° C.).

出典と根拠

ORDレコード: ord-174a97b9133e4ebebd6746a8bdd55a63
出典データセット: uspto-grants-2000_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06096782

反応ノート

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