4-Bromo-2-methylaniline → 4'-Amino-2,3'-dimethylbiphenyl-4-carboxylic acid

HRID 1870890

反応式

HRID 1870890 の反応式
Br[C:2]1[CH:8]=[CH:7][C:5]([NH2:6])=[C:4]([CH3:9])[CH:3]=1.B([C:13]1[CH:21]=[CH:20][C:16]([C:17]([OH:19])=[O:18])=[CH:15][C:14]=1[CH3:22])(O)O>>[NH2:6][C:5]1[CH:7]=[CH:8][C:2]([C:13]2[CH:21]=[CH:20][C:16]([C:17]([OH:19])=[O:18])=[CH:15][C:14]=2[CH3:22])=[CH:3][C:4]=1[CH3:9]

参加物

3

反応物 2

HCID 114234-Bromo-2-methylanilineHCID 221158924-Borono-3-methylbenzoic acid

生成物 1

HCID 186942714'-Amino-2,3'-dimethylbiphenyl-4-carboxylic acid

実験手順

The title compound was prepared from 4-bromo-2-methylaniline and 4-borono-3-methylbenzoic acid (D29) using a similar procedure to Description 1 as a brown solid (41%). This was used in the next step without further purification.

後処理

  1. customThis was used in the next step without further purification

出典と根拠

ORDレコード
ord-3834fa6b35b140f99b470d78d13eaf95
出典データセット
uspto-grants-2000_08
特許番号
US06100272

関連ノート

読み込み中…