N-Ethylaniline → ethyl 3-(4-benzyloxyphenyl)-2-(phenyl-N-ethylamino)propionate
反応式
[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([CH2:15][CH:16](OS(C)(=O)=O)[C:17]([O:19][CH2:20][CH3:21])=[O:18])=[CH:11][CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:27]([NH:29][C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1)[CH3:28]>>[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([CH2:15][CH:16]([N:29]([C:30]2[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=2)[CH2:27][CH3:28])[C:17]([O:19][CH2:20][CH3:21])=[O:18])=[CH:11][CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1参加物
3
実験手順
Reaction and post-treatment were carried out according to Reference example 5(a) using 4.50 g of ethyl 3-(4-benzyloxyphenyl)-2-methanesulfonyloxypropionate and 5.6 ml of N-ethylaniline to obtain 6.30 g of a mixture of the desired compound and N-ethylaniline as a syrup.
後処理
- customReaction
出典と根拠
- ORDレコード
- ord-3a02a7f654584c11a76592875a3c0d1a