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Water → 15beta,16beta-Methylene-3-methoxyandrosta-3,5-diene-17-one

HRID 1876737
ノート
印刷プレビュー

反応式

HRID 1876737 の反応式
[I-].[CH3:2][S+](C)(C)=O.[OH-].[K+].C(O[C@@H:13]1[C@H:18]2[C@H:19]3[C@H:29]([CH2:30][CH2:31][C@:16]2([CH3:17])[C:15](=[O:34])[CH2:14]1)[C@:27]1([CH3:28])[C:22]([CH:23]=[C:24]([O:32][CH3:33])[CH2:25][CH2:26]1)=[CH:21][CH2:20]3)(=O)C.O>CS(C)=O>[CH2:2]1[C@@H:14]2[C:15](=[O:34])[C@:16]3([CH2:31][CH2:30][C@H:29]4[C@@H:19]([CH2:20][CH:21]=[C:22]5[C@:27]4([CH3:28])[CH2:26][CH2:25][C:24]([O:32][CH3:33])=[CH:23]5)[C@@H:18]3[C@H:13]12)[CH3:17]
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

6

反応物 4

HCID 962WaterHCID 14797Potassium HydroxideHCID 74498Sulfoxonium, trimethyl-, iodide (1:1)HCID 54571005(15alpha)-15-(Acetyloxy)-3-methoxyandrosta-3,5-dien-17-one

生成物 1

HCID 1403164815beta,16beta-Methylene-3-methoxyandrosta-3,5-diene-17-one

試薬・触媒・溶媒 1

HCID 679
Dimethyl Sulfoxide
溶媒

反応条件

温度
27.5 °C

実験手順

12.96 kg of trimethylsulfoxonium iodide is dissolved in 180 l of dimethyl sulfoxide under nitrogen bubbling and vigorous stirring and at 25-30° C. 5.51 kg of potassium hydroxide is added to the solution. Stirring is continued for 1 hour, then 16.22 kg of 15α-acetoxy-3-methoxyandrosta-3,5-diene-17-one is added, the reaction mixture is stirred at 25-30° C. until the reaction is complete (about 6 hours). The solution is added slowly to 900 l of water, the precipitate obtained is stirred for 30 minutes until it is dense, filtered by centrifuge, washed with portions of water until is neutral and dried in vacuo to constant weight at a temperature below 40° C. and the crude tide compound is crystallized from methanol.

後処理

  1. stirringStirring
  2. stirringthe reaction mixture is stirred at 25-30° C. until the reaction
  3. custom(about 6 hours)
  4. customthe precipitate obtained
  5. stirringis stirred for 30 minutes until it
  6. filtrationfiltered by centrifuge
  7. washwashed with portions of water
  8. customdried in vacuo to constant weight at a temperature below 40° C.
  9. customthe crude tide compound is crystallized from methanol

出典と根拠

ORDレコード
ord-49ad37c4f9d043ebbf1a289c2e247868
出典データセット
uspto-grants-2012_11
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US08309712B2

反応ノート

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