化工社化工社 化学情報印刷レポート · 研究参考用
2-Ethyl-5-[4-(trifluoromethyl)phenyl]-3-furaldehyde → 1-{2-Ethyl-5-[4-(trifluoromethyl)phenyl]-3-furyl}-3-methylbutan-1-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Ethyl-5-[4-(trifluoromethyl)phenyl]-3-furaldehyde | HCID 23074355 | — |
| 反応物 | HCID 178420648 | HCID 178420648 | — |
| 生成物 | 1-{2-Ethyl-5-[4-(trifluoromethyl)phenyl]-3-furyl}-3-methylbutan-1-ol | HCID 68513344 | 83% |
反応手順
An operation similar to that in Example 3 (2) was performed using 2-ethyl-5-[4-(trifluoromethyl)phenyl]-3-furaldehyde (805 mg) and 1N isobutylmagnesium bromide-tetrahydrofuran solution (6.0 mL) to give the title compound (819 mg, 83%) as an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08309580B2 |
| 出典データセット | uspto-grants-2012_11 |
| ORD ID | ord-f48eec13cb6e43389fa47c6a5b98254b |
| 出典メモ | uspto-grants-2012_11 |